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A practical, recyclable strategy for homogeneous cinchona alkaloid‐derived primary amine organocatalysts was developed by controlling the solubilities in an aqueous/organic biphasic system through regulating the pH of the aqueous phase, effecting the protonation and deprotonation of primary amino, tertiary amino and pyridyl groups. By means of model aldol, vinylogous Michael and double‐Michael cascade...
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