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Developing high‐efficiency electrocatalysts for hydrogen evolution reaction (HER) is vitally important in electrochemical water splitting technology. Herein, ultra‐small Ni‐doped CuCo2S4 nanoparticles (NCCS NPs) are easily achieved in a single step by a facile hydrothermal method. The investigations, using powder X‐ray diffraction, X‐ray photoelectron spectroscopy, scanning electron microscopy, and...
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