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Monolayer WO3·H2O (ML‐WO3·H2O) nanosheets are synthesized via a space‐confined strategy, and then a single‐atom catalyst (SAC) is constructed by individually immobilizing Pt single atoms (Pt‐SA) on monolayer WO3 (ML‐WO3). The Pt‐SA/ML‐WO3 retains the monolayer structure of ML‐WO3·H2O, with a quite high monolayer ratio up to ≈93%, and possesses rich defects (O and W vacancies). It exhibits excellent...
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