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The formation of the P‐cyclohexyl dinitrogen complex, (CyPh[NPN]Ta)2(μ‐η2:η1‐N2)(μ‐H)2 (CyPh[NPN] = [CyP(CH2SiMe2NPh)2], and Cy = C6H11) is described and its reaction with butylsilane (BuSiH3) explored. The reaction was monitored by multinuclear NMR spectroscopy and showed the formation of a number of intermediates. The final product is a hydride‐bridged imido‐amido silyated species that has the imido...
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