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Novel cyclodextrin (CD) chiral stationary phases (CD‐CSPs) with well‐defined structure have been successfully synthesized by immobilization of mono/di(10‐undecenoyl)‐perphenylaminocarbonyl β‐CD on the 3‐mercaptopropyl functionalized silica gel via thiol‐ene click chemistry. The phenyl carbamate groups on the rims of CD extended the cavity of CD‐CSPs, which facilitated the formation of inclusion complex...
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