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Dimethoxymethane was first synthesized from methanol with a liquid phase intermittent process which only used molecular oxygen as the sole oxidant. RuCl3 was proved to be an efficient catalyst as it posses the ability of oxidizing methanol and Lewis acidic which promotes the oxidation of methanol to formaldehyde and then methanol condensed with formaldehyde to form dimethoxymethane at Lewis acid site.
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