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Pure body-center-cubic structured metastable polycrystalline Li 15 Si 4 was synthesized in a Li-ion battery by electrochemically lithiating a thin Si wafer. Its stability and compressional behavior were investigated using in-situ high-pressure synchrotron X-ray diffraction (XRD) at room temperature. No phase transition was observed in polycrystalline Li 15 Si 4 up to...
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