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Hemi-hydrate and anhydrous CaSO4 whiskers with adjustable aspect ratio were continuously synthesized by the reactive crystallization of CaCl2 to K2S2O8 in microdroplets. The effects of solvent and reactive temperature were examined, with SEM and XRD characterizations. Hemi-hydrate and anhydrous CaSO4 whiskers can be, respectively, obtained in aqueous and N,N-dimethylformamide solutions at 90°C in...
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