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A fcc nanoporous palladium (NP Pd) with a pore size of ∼2nm and ligament size of ∼4nm is obtained after electrochemical dealloying an amorphous Pd 42.5 Cu 30 Ni 7.5 P 20 precursor in a 0.1moldm −3 H 2 SO 4 solution at constant current densities of 17mAcm −2 for 12ks. A nanoporous Pd–P solid solution forms at lower currents. The cyclic...
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