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A soluble metal-free phthalocyanine 5 and its metal complexes (Zn, Ni, Co and Cu) 6, 7, 8 and 9 containing eight 16-membered tetrathiamonoaza macrocycles on peripheral substituent positions have been synthesized. The metal-free phthalocyanine 5 was synthesized from 4,5-bis{[2-(1,4,10,13-tetrathia-7-azacyclohexadecan-7-yl)ethyl]oxy}phthalonitrile 4. The metal complexes 6, 7 and 8 were prepared by a...
Novel metal-free and metal-containing (Zn, Ni, Cu) derivatives bearing eight 16-membered tetrathiamonoaza macrocycles in peripheral positions were synthesized and characterized by a combination of elemental analysis, UV–vis, FT-IR, NMR and MS spectral data. The metal-free phthalocyanine was synthesized by two different routes namely from 4,5-bis{[2-(1,4,10,13-tetrathia-7-azacyclohexadecan-7-yl)ethyl]thio}phthalonitrile...
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