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A series of single phase LiNi(1−x)CuxPO4 (0 < x < 0.99) was successfully synthesized by non-aqueous sol–gel method followed by microwave (MW) annealing. The advantage of MW short span annealing is obvious from the nanometer sized particles compared to reported microparticles. XRD, IR and SEM studies were conducted to investigate the phase purity, crystal structure, lattice parameters and morphology...
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