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Novel ZrV2O7 microfibers with diameters about 1–3μm were synthesized using a sol–gel technique. For comparison, ZrV2O7 powders were prepared by the same method. The resultant structures were studied by X-ray diffraction, field-emission scanning electron microscopy and transmission electron microscopy. The results indicated that both the pure ZrV2O7 microfibers and powders could be synthesized by the...
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