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This paper reports on the self-branching of TiO2 nanotubes during anodization of Ti metal carried out at a fixed applied potential. These nanotubes are prepared by a two-step anodization carried out in an aqueous electrolyte containing ethylene glycol and ammonium fluoride at a range of anodization voltages of 30–60 V. The self-branching of nanotubes is more pronounced in the first-step anodization...
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