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A UV‐induced 1,3‐dipolar nucleophilic addition of tetrazoles to thiols is described. Under UV irradiation the reaction proceeds rapidly at room temperature, with high yields, without a catalyst, and in both polar protic and aprotic solvents, including water. This UV‐induced tetrazole‐thiol reaction was successfully applied for the synthesis of small molecules, protein modification, and rapid and facile...
Wir beschreiben ein neues UV‐initiiertes Verfahren, das eine direkte Funktionalisierung von oberflächengebundenen Hydroxygruppen mit Thiolen ermöglicht (hier als Thiol‐Alkohol‐Modifizierung bezeichnet). Diese Methode beruht auf einer oxidativen Kupplung von Thiol‐ an Hydroxygruppen. Wir zeigen, dass verschiedene Moleküle, die Thiolgruppen tragen, z. B. Fluorophore, thiolterminiertes Polyethylenglycol...
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