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The cluster [Ir11(CO)23]3− was obtained by reaction of [Ir10(CO)21]2− and [Ir(CO)4]− in refluxing MeCN, and its solid-state structure was determined on the salt [NEt4]3[Ir11(CO)23]. The metallic framework of D3h symmetry is composed by three face-fused octahedra, all sharing a common edge. The cluster contains 9 edge bridging and 14 terminal carbonyl ligands, a disposition different from that of the...
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