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It is significant to investigate the effect of aluminum (Al) on the thermal activity of Dihydroxylammonium 5, 5′‐bistetrazole‐1, 1′‐diolate (TKX‐50) for the application of TKX‐50‐based composite solid propellant. In this work, TKX‐50/Al composites with different particle sizes and contents of Al were blended, and the thermal decomposition and combustion properties were investigated by differential...