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This study presents for the first time an NMR spectroscopic characterization of the room and high temperature phases of (NH 4 ) 3 InF 6 using 19 F and 115 In as probe nuclei. The reversible phase transition to the cubic phase at 353K was followed by MAS NMR in situ. Static NMR experiments of the room temperature phase and MAS NMR experiments of the high temperature...
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