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The ternary antimonide CeNiSb 3 has been prepared from an Sb flux or from reaction of Ce, NiSb, and Sb above 1123K. It crystallizes in the orthorhombic space group Pbcm with Z=12 and lattice parameters a=12.6340(7)A, b=6.2037(3)A, and c=18.3698(9)A at 193K. Its structure consists of buckled square nets of Sb atoms and layers of highly distorted edge- and face-sharing NiSb 6 octahedra...
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