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Amphiphilic double poly(ionic liquid) (PIL) block copolymers are directly prepared by cobalt‐mediated radical polymerization induced self‐assembly (CMR‐PISA) in water of N‐vinyl imidazolium monomers carrying distinct alkyl chains. The cobalt‐mediated radical polymerization of N‐vinyl‐3‐ethyl imidazolium bromide (VEtImBr) is first carried out until high conversion in water at 30 °C, using an alkyl...
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