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Samples of Zintl phase YbCd2–xMnxSb2 (CaAl2Si2‐type, space group P$\bar {3}$m1) were prepared by a solid‐state reaction followed by a suitable annealing and spark plasma sintering (SPS) for densification. Investigations were carried out on chemical substitution of Cd by Mn in order to optimize the thermoelectric figure of merit ZT in the solid solution system YbCd2–xMnxSb2 (x = 0, 0.05, 0.1, 0.15,...
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