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The direct electrosynthesis of neutral copper(II) and zinc(II) complexes of a new unsymmetrical carboxamide ligand, N,N′-bis(2-pyridinecarboxamide)-2-aminobenzylamine (H 2 bpabza) derived from 2-pyridinecarboxylic acid and 2-aminobenzylamine, was accomplished by electrochemical oxidation of anodic metals (copper and zinc) in an acetonitrile solution of the ligand. These compounds were characterized...
Three novel complexes of zinc with hexadentate amide–thioether ligands were synthesized by electrochemical oxidation of zinc in dichloromethane–methanol solution. These compounds were characterized by elemental analyses, 1 H NMR, and IR spectroscopy. The molecular structures of two complexes were determined by single crystal X-ray diffraction, indicating that, the metal atom is in a distorted...
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