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Ein chemoselektives und robustes Protokoll zur γ‐Oxidation von β,γ‐ungesättigten Amiden wird dargelegt. Bei dieser Methode ermöglicht elektrophile Amidaktivierung eine bei ungesättigten Amiden bisher selten angewendete regioselektive Reaktion mit TEMPO, die zu γ‐aminoxylierten α,β‐ungesättigten Amiden führt. Radikalische Zyklisierungen und Oxidationen der synthetisierten Produkte untermauern die Nützlichkeit...
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