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Capillary liquid chromatography (LC) is used for the determination of tocopherols and tocotrienols in cosmetic products. Dispersive liquid–liquid microextraction (DLLME) allows the analytes to be preconcentrated into a very small volume of organic solvent which is then injected into the chromatograph running at a very low flow rate. Pressurized liquid extraction (PLE) at a high temperature and pressure...
Pressurized liquid extraction (PLE) and dispersive liquid–liquid microextraction (DLLME) were used to isolate and preconcentrate tocopherols and tocotrienols from plant foods. The Taguchi experimental method was used to optimize the six factors (three levels for each factor), affecting DLLME, namely: carbon tetrachloride volume, methanol volume, aqueous sample volume, pH of sample, sodium chloride...
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