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The high temperature phase transformations of zirconium were investigated by “in-situ” X-ray diffraction analysis. The experiments were carried out in a high temperature chamber Anton Paar HTK 1200N mounted on powder diffractometer Panalytical X’Pert Pro. The chamber was evacuated by a turbo-molecular pump creating a pressure about 3 × 10 −4 Pa at the temperature 1200 °C before the measurement...
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