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Iron tri(hydrogenphosphite), Fe(HPO3H)3, crystallizes in both a monoclinic and a hexagonal space group. In this report the structure determination of the hexagonal variant is described: space group P63, a = 8.1690(2) Å, c = 6.9300(2) Å. The structure is slightly disordered, Fe3+ being partially replaced by Al3+, and is very close to that of Fe2(HPO3)3. The only significant difference is that one half...
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