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Comparative studies using high temperature in situ Raman spectroscopy, TPSR, pulsed reactions of CH 4 , H 2 -TPR and O 2 -TPD techniques were carried out on Rh/Al 2 O 3 calcined at 600 and 900°C to elucidate the effect of calcination temperatures on the nature of the Rh species in the catalysts and its relationship with the catalytic performance of Rh/Al ...
In situ time-resolved FTIR spectroscopy was used to study the reaction mechanism of partial oxidation of methane to synthesis gas and the interaction of CH 4 /O 2 /He (2/1/45) gas mixture with adsorbed CO species over SiO 2 and γ-Al 2 O 3 supported Rh and Ru catalysts at 500-600 o C. It was found that CO is the primary product for the reaction of CH...
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