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As part of a strategy to explore highly functionalized macromolecular semiconductors, a series of highly substituted twelve‐armed macromolecules F1CzTr‐F3CzTr consisting of truxene, 9‐phenylcarbazole and oligofluorene units were synthesized. To accomplish the synthesis of twelve‐armed targets, a high yield microwave enhanced synthesis method for direct twelve‐fold Suzuki couplings was developed. The...
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