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High alkaline desilication solution (DSS), a high volume byproduct from the pretreatment of high‐alumina fly ash, was used as low‐cost mother liquor for the synthesis of calcium silicate hydrate (C‐S‐H). Through the combined analysis of X‐ray diffraction, thermogravimetric analysis, X‐ray fluorescence, 29Si MAS NMR, and Brunauer‐Emmett‐Teller, the relationship between chemical composition and structure...
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