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The bimetallic NiSn2 complex Ni(SnBu 3t )2(CO)3,1, was obtained from the reaction of Ni(COD)2 and Bu 3t SnH and CO. The reaction of Co2(CO)8 and Bu 3t SnH afforded the bimetallic Co–Sn complex Co(SnBu 3t )(CO)4, 3. Compound 3 was also obtained from the reaction of Co4(CO)12 and Bu 3t SnH but in a lower yield. Both compounds 1 and 3 were characterized by single crystal X-ray diffraction, and...
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