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We report a strategy for regulating the rate of internally bound anion exchange within an Fe4L6 metal–organic tetrahedron through external coordination of tripodal tris(alkylammonium) cations. The cage features three flexible 18‐crown‐6 receptors at each of its FeII vertices, facilitating strong tritopic interactions with tris(ammonium) cations to “cap” the vertices of the tetrahedron. This capping...
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