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Solvothermal reaction of Cd(OAc)2·2H2O and biphenyl-2,3,3′,5′-tetracarboxylic acid (H4bptca) in DMF/H2O afforded one novel coordination polymer [Cd4(bptca)2(DMF)4]n (1). X-ray structural analysis reveals that complex 1 is a chiral bilayer supported by rare asymmetrical tetranuclear [Cd4(μ3-O)2(μ2-O)]. Topologically, the net can be considered as a 3,6-connected Shubnikov plane with the Schläfli symbol...
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