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A new single‐urea‐bound chiral stationary phase based on 3,5‐dimethylphenylcarbamoylated β‐cyclodextrin was prepared through the Staudinger reaction of mono (6A‐azido‐6A‐deoxy)‐per(3,5‐dimethylphenylcarbamoylated) β‐cyclodextrin and 3‐aminopropyl silica gel under CO2 atmosphere. The new phase exhibited good enantioseparation performance for 33 analytes using normal‐phase HPLC conditions; 19 of them...
DOI: 10.1002/elps.201700273
The cover picture shows chiral separations of racemic analytes on a new single‐urea‐bound β‐cyclodextrin chiral stationary phase by HPLC. This new CSP was prepared through the Staudinger reaction of β‐cyclodextrin derivative and 3‐aminopropyl silica gel under CO2 atmosphere. It exhibited good separation performance for 33 analytes using normal‐phase HPLC conditions. Effects...
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