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Acylation of ferrocene by an acylating agent generated in situ from the corresponding carboxylic acid and phosphorus trichloride, in the presence of the catalyst generated electrochemically from a sacrificial aluminum anode, was investigated. The corresponding monoacylferrocenes were obtained in very high yields when the molar ratio of reactants was ferrocene/carboxylic acid/PCl 3 =1:1.2:1,...
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