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A gold‐catalyzed cyclization/cascade skeletal rearrangement of o‐cyanophenylalkynones with 3‐amino‐benzo[d]‐isoxazoles has been developed, which provides an approach for synthesizing medium‐sized benzolactones. Based on the experimental results, we postulate that the initial nucleophilic attack occurs preferentially at the keto moiety instead of the gold‐carbene. This reactivity initiates an attractive...
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