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In the past decade, considerable progress has been made in the understanding of catalytic systems which simultaneously possess both mononuclear and dinuclear intermediates. The present contribution begins by reviewing the necessary background concerning stoichiometric binuclear elimination. This is followed by a summary of in situ FTIR studies on corresponding homometallic and hetero-bimetallic catalytic...
The homogeneous catalytic hydroformylation of 3,3-dimethylbut-1-ene was studied, starting with Rh 4 (σ-CO) 9 (μ-CO) 3 as catalyst. The multiple experiment in situ spectroscopic data were preconditioned to subtract the absorbance due to background moisture, carbon dioxide, and solvent. The preconditioned data were then subjected to band-target entropy minimization (BTEM) in...
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