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Deuteriopolystyrene of molecular weight ca 32 000 g mol -1 has been functionalized at one end with a fluorocarbon. On mixing this polymer with an unfunctionalized hydrogenous polystyrene a surface excess layer of the deuteriopolymer forms on annealing at 423 K. The surface excess as a function of deuteriopolymer content has been obtained using nuclear reaction analysis and neutron reflectometry,...
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