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4 -Deoxy-α-maltosyl fluoride and 4 -deoxy-α-maltotriosyl fluoride were synthesized to serve as mechanistic probes for α-glucanotransferases such as the glycogen debranching enzyme. The deoxy derivatives were prepared starting from maltose and maltotriose, respectively. Deoxygenation of the terminal 4-hydroxyl group was accomplished by radical reduction of the iodo sugar formed after iodide displacement...
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