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Gd 5 CoSi 2 was prepared by annealing at 1003K. Its investigation by the X-ray powder diffraction shows that the ternary silicide crystallizes in a tetragonal structure deriving from the Cr 5 B 3 -type (I4/mcm space group; a=7.5799(4) and c=13.5091(12)Å as unit cell parameters). The Rietveld refinement shows a mixed occupancy on the (8h) site between Si and Co atoms...
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