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A novel process for the direct ammoxidation of propane over steam-activated Fe-silicalite at 723–823 K is reported. Yields of acrylonitrile (ACN) and acetonitrile (AcCN) below 5% were obtained using N2O or O2 as the oxidant. Co-feeding N2O and O2 boosts the performance of Fe-silicalite compared to the individual oxidants, leading to AcCN yields of 14% and ACN yields of 11% (propane conversions of...
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