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Composite nickel/thallium hexacyanoferrates were prepared as thin films on electrode surfaces. Electrodeposition of composite films was achieved by potential cycling in the solution for modification containing, in addition to potassium salt electrolyte, nickel(II), thallium(I), and hexacyanoferrate(III). Depending on the relative amounts of thallium to nickel, either a mixed phase with respect to...
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