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By depositing nanorods of tungsten oxide over catalytic palladium nanoparticles (dispersed onto glassy carbon substrate), enhancement of the overall electrocatalytic activity toward oxidation of formic acid in acid medium was observed. The effect was particularly evident from the increase of chronoamperometric currents at a fairly low potential of 0.04V vs. RHE. Under such conditions, tungsten oxide...
We demonstrate the usefulness of cyclic voltammetric measurements for characterization of a model, mixed-valence protonically conducting solid, tetragonal phospho-12-tungstic acid single crystal, H 3 PW 12 O 40 29H 2 O, in the absence of liquid electrolyte phase. The measurements were performed in an all-solid cell which utilizes a carbon fiber ultramicrodisk...
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