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The problem at hand is the electrochemical oxidation of oxalate ion, which is accelerated by fluoride ion at a platinum anode. The hypothesis that fluoride ion traps incipient hydroxyl radicals as hydroxyfluoride radical anions was not supported by ESR experiments in which hydroxyl radicals were generated in the presence of the spin trap α-(4-pyridyl-1-oxide) N-tert-butyl-nitrone with and without...
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