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The single enantiomer drug, alogliptin (Alo, Nesina®) is a novel, orally available and selective dipeptidyl peptidase‐4 inhibitor used for the treatment of type II diabetes. Following its pKa determination by CE‐pH titration, a validated chiral CE method has been developed to separate Alo enantiomers. Preliminary screening of the native CDs and their ten derivatives revealed that sulfopropylated‐γ‐CD,...
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