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The surface reactions of CCl 4 with the Fe 3 O 4 (111)-(2x2) selvedge of naturally occurring α-Fe 2 O 3 (0001) single-crystals have been investigated using synchrotron X-ray photoelectron spectroscopy (XPS) and temperature-programmed desorption (TPD). CCl 4 was found to dissociate on the Fe 3 O 4 surface at 100 K producing chemisorbed...
Temperature programmed reaction/desorption (TPR/D) studies were undertaken to characterize the surface chemistry which occurs between CCl 4 and the Fe 3 O 4 (111) selvedge of single crystal α-Fe 2 O 3 (0001). Six separate desorption events are clearly observed and four desorbing species are identified: CCl 4 , OCCl 2 , C 2 Cl 4 ...
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