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We explored routes for the synthesis of LiMn2O4 spinel from five different polymorphs of MnO2 as the manganese source. These included α and β-MnO2 and three types of γ MnO2 (electrochemically produced EMD, and two types of chemically produced CMD). The synthesis included a lithiation step by mild reduction of the MnO2 with glucose in a LiOH solution, followed by calcination of the lithiated product...
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