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The alkali metal‐nickel carbonyl anions ENi(CO)3− with E=Li, Na, K, Rb, Cs have been produced and characterized by mass‐selected infrared photodissociation spectroscopy in the gas phase. The molecules are the first examples of 18‐electron transition metal complexes with alkali atoms as covalently bonded ligands. The calculated equilibrium structures possess C3v geometry, where the alkali atom is located...
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