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The reactivity of the sulfur‐containing nucleoside 4‐thio‐(2′‐deoxy)‐thymidine usually abbreviated as 4‐thio‐thymidine, (S4‐TdR) under Fenton conditions, ie, in the presence of H2O2 and catalytic amounts of Fe(II), was investigated by UV‐vis spectroscopy and electrospray ionization single and tandem mass spectrometry (ESI‐MS and MS/MS). S4‐TdR hydroxylated on the S atom was found to be a key reaction...
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