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High loadings of 12-tungstophosphoric acid (H3PW12O40) were incorporated within highly porous metal-organic framework MIL-101. The samples have been characterized using different techniques such as XRD, TEM, FT-IR, TGA, N2 adsorption and Raman spectroscopy. XRD and TEM did not show any aggregation of the H3PW12O40 nanocrystals on the surface of MIL-101 crystals up to 70wt%. Similarly, N2 sorption–desorption...
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