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Electrochemical scanning tunneling microscopy was used to study the structural evolution of adsorbed CO during preoxidation on Pt(111) modified with spontaneously deposited Ru. During the preoxidation process, a phase transition was observed from (2×2)-3CO-α to (√19×√19)R23.4°-13CO via the transient structures (2×2)-3CO-β and (1×1)-CO. A comparison of these structural changes with those that occur...
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