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Sphere‐like Fe3O4 aggregates were solvothermally prepared with ethylene glycol, sodium acetate and FeCl3·6H2O as raw materials. The sphere‐like Fe3O4 aggregates provided heterogeneous growth sites for Au nanoparticles. These were obtained by reduction of HAuCl4 by sodium citrate under mild reaction conditions and the Fe3O4‐Au nanocomposites were subsequently formed. The peroxidase‐like activity of...
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